5 - Amino - 3 - methyl - 1 , 2 , 4 - thiadiazole

نویسندگان

  • R. Alan Aitken
  • Alexandra M. Z. Slawin
چکیده

An improved procedure for isolation of 5-amino-3-methyl-1,2,4-thiadiazole in pure form on a multi-gram scale without chromatography is reported. Its 1H and 13C-NMR and IR data are presented and previously published erroneous data corrected. The molecular structure is confirmed by X-ray diffraction which shows layers consisting of an elaborate two-dimensional hydrogen bonded network of molecules.

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تاریخ انتشار 2018